GDX-102填充柱測甲醇和醇 蒸餾酒與配制酒衛生標準的分析方法
產品名稱:GDX-102填充柱測甲醇和醇 蒸餾酒與配制酒衛生標準的分析方法
產品型號:GDX-102填充柱測甲醇和醇
產品廠商:浩瀚色譜(山東)應用技術開發有限公司
簡單介紹
蒸餾酒與配制酒衛生標準的分析方法,液化石油氣,二甲醚,甲縮醛,乙縮醛,乙醇,室內空氣,焦爐煤氣,煉廠氣,天然氣,變壓器油,多氯聯苯,植物油,6號溶劑殘留,裂解進樣器
GDX-102填充柱測甲醇和醇 蒸餾酒與配制酒衛生標準的分析方法的詳細介紹
蒸餾酒與配制酒衛生標準的分析方法
蒸餾酒與配制酒衛生標準的分析方法 詳細信息:
名稱:填充柱
蒸餾酒與配制酒衛生標準的分析方法 詳細信息:
名稱:填充柱
載體:GDX-102(60-80目),氣相色譜用?;蛏显?402有機擔體,60^-80目。
蒸餾酒與配制酒衛生標準的分析方法 測試譜圖:
Analytical methods for the hygienic standards of distilled liquor and mixed liquor
Analytical methods for the hygienic standards of distilled spirits and blended spirits Details:
Name: Packed column
Carrier: GDX-102 (60-80 mesh) for gas chromatography. Or test 402 organic carrier, 60^-80 mesh.
Chromatographic column: length 2m, inner diameter 4mm, glass column or stainless steel column.
Application: GB/T 5009.48-1996 Analytical method of hygienic standards for distilled and mixed liquors
GB/T 5009.48-2003 Method for analysis of hygienic standards for distilled and mixed liquors
4.4 Methyl alcohol and higher alcohols (determined by gas chromatography)
441 Principle
The chemical io nization of different alcohols in a hydrogen flame is used for detection, and the peak height is compared with the standard. Minimum mark limit: Zheng Bing drunk, Zheng
Butanol 0.Zng, isoamyl alcohol, n-pentanol 0.15ng; seco ndary T alcohol, iso-T alcohol 0.22ng.
4.4.2 Reagents
4.4.3 Apparatus
44.3.1 Gas chromatograph: with hydrogen flame io nization detector.
4.4-3.2 Micro injection syringe: 1ul, 50ulL,
4.4.4 Analysis steps
4.4.4.1 Chromatographic reference conditions
4.4.4.1.1
Chromatographic column: length 2m, inner diameter 4mm, glass column or stainless steel column.
4.4.4.1.2
Statio nary phase: GDX-102,
60^-80 mesh. Or test 402 organic carrier, 60^-80 mesh.
4.4.4.1.3 Vaporization chamber temperature: 1900C,
4.4.4, .4 Detector temperature: 1900C,
4.4.4.1.5 Column temperature: 1700c,
4.4.4.1.6 Carrier gas (N2) flow rate: 40mL/min,
4.4.4.1.7 Hydrogen (H,) flow rate: 40mL/min,
4.4.4.1.8 Air flow rate: 450mL/min.
4.4.4., 9 Injection volume: 0.5ul
Analytical methods for the hygienic standards of distilled spirits and blended spirits Test spectrum:
色譜柱:長 2m,內徑4mm,玻璃柱或不銹鋼柱。
應用:GB/T 5009.48-1996 蒸餾酒與配制酒衛生標準的分析方法
GB/T 5009.48-2003 蒸餾酒與配制酒衛生標準的分析方法應用:GB/T 5009.48-1996 蒸餾酒與配制酒衛生標準的分析方法
4.4 甲醉和醇類(氣相色譜法測定)
441 原理
利用不同醇類在氫火焰中的化學電離進行檢測,根據峰高與標準比較定童。低標出限:正丙醉、正
丁醇0.Zng,異戊醇、正戊醉0.15ng;仲T醉、異T醇0.22ng。
4.4.2 試劑
4.4.3 儀器
4.4-3.2 微量進樣注射器:1ul,50ulL,
4.4.4 分析步驟
4.4.4.1 色譜參考條件
4.4.4.1.1
色譜柱:長 2m,內徑4mm,玻璃柱或不銹鋼柱。
4.4.4.1.2
固定相:GDX-102,
60^-80目?;蛏显?402有機擔體,60^-80目。
4.4.4.1.3汽化室溫度:1900C,
4.4.4,.4檢測器溫度:1900C,
4.4.4.1.5柱溫:1700c,
4.4.4.1.6 載氣(N2)流速:40mL/min,
4.4.4.1.7 氫氣(H,)流速:40mL/min,
4.4.4.1.8 空氣流速:450mL/min.
4.4.4.,,9 進樣量:0.5ul
蒸餾酒與配制酒衛生標準的分析方法 測試譜圖:
Analytical methods for the hygienic standards of distilled liquor and mixed liquor
Analytical methods for the hygienic standards of distilled spirits and blended spirits Details:
Name: Packed column
Carrier: GDX-102 (60-80 mesh) for gas chromatography. Or test 402 organic carrier, 60^-80 mesh.
Chromatographic column: length 2m, inner diameter 4mm, glass column or stainless steel column.
Application: GB/T 5009.48-1996 Analytical method of hygienic standards for distilled and mixed liquors
GB/T 5009.48-2003 Method for analysis of hygienic standards for distilled and mixed liquors
4.4 Methyl alcohol and higher alcohols (determined by gas chromatography)
441 Principle
The chemical io
Butanol 0.Zng, isoamyl alcohol, n-pentanol 0.15ng; seco
4.4.2 Reagents
4.4.3 Apparatus
44.3.1 Gas chromatograph: with hydrogen flame io
4.4-3.2 Micro injection syringe: 1ul, 50ulL,
4.4.4 Analysis steps
4.4.4.1 Chromatographic reference conditions
4.4.4.1.1
Chromatographic column: length 2m, inner diameter 4mm, glass column or stainless steel column.
4.4.4.1.2
Statio
60^-80 mesh. Or test 402 organic carrier, 60^-80 mesh.
4.4.4.1.3 Vaporization chamber temperature: 1900C,
4.4.4, .4 Detector temperature: 1900C,
4.4.4.1.5 Column temperature: 1700c,
4.4.4.1.6 Carrier gas (N2) flow rate: 40mL/min,
4.4.4.1.7 Hydrogen (H,) flow rate: 40mL/min,
4.4.4.1.8 Air flow rate: 450mL/min.
4.4.4., 9 Injection volume: 0.5ul
Analytical methods for the hygienic standards of distilled spirits and blended spirits Test spectrum:
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